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Abstract
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This research is of significant necessity and importance as it addresses critical challenges in environmental and analytical chemistry while aligning with global sustainability goals. Phenolic acids, although valuable bioactive compounds, become pollutants when present in high concentrations, posing risks to aquatic ecosystems and drinking water resources. Traditional extraction techniques, such as LLE and SPE, face limitations due to their high solvent consumption, inefficiency in handling low analyte concentrations, and inability to process complex sample matrices effectively. These challenges highlight the urgent need for innovative and scalable solutions. By leveraging 3D printing technology to develop advanced adsorbents, this research introduces a cutting-edge, environmentally friendly approach to enhance the sensitivity, selectivity, and reusability of microextraction methods. Such advancements not only improve analytical precision but also contribute to effective environmental monitoring, food safety protocols, and public health initiatives. Moreover, the sustainable design of these adsorbents, which minimizes solvent use and promotes reusability, aligns with the global demand for greener scientific practices. The research thus holds broad applicability, offering transformative solutions for environmental surveillance, industrial pollution management, and the advancement of analytical chemistry..
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